المؤلفون: Egorov Vladimir, Svetlana N. Sytova, Yauheni Shauchenka, Alexander Kolesnov, Lidia Sobolenko, Anton N. Kavalenka, Siarhei V. Charapitsa, Sergey M. Leschev, Natalia Zayats, Sergey Vetokhin, Nikolai Kostyuk, Sergey Tsimbalaev

المصدر: Food Analytical Methods. 14:2088-2100

مصطلحات موضوعية: Volatiles, Methyl acetate, Ethyl acetate, Alcohol, Acetaldehyde, метанол, Ethanol fermentation, ацетальдегид, 01 natural sciences, Applied Microbiology and Biotechnology, Analytical Chemistry, chemistry.chemical_compound, 0404 agricultural biotechnology, эталонное вещество, Safety, Risk, Reliability and Quality, летучие вещества, Reference substance, Ethanol, Chromatography, Methanol, 010401 analytical chemistry, алкогольные напитки, 04 agricultural and veterinary sciences, Repeatability, 040401 food science, 0104 chemical sciences, chemistry, Alcoholic beverages, Safety Research, этанол, Food Science

الوصف: The article presents the results of collaborative study of the method for gas chromatographic determination of alcoholic fermentation volatile by-products (acetaldehyde, methanol, methyl acetate, ethyl acetate, propan-2-ol, propan-1-ol, 2-methylpropan- 1-ol, butan-1-ol, and 3-methylbutan-1-ol) in alcoholic beverages with volume ethanol content in a range of 9.9–96.0% (wine, sake, liquor, tequila, vodka, grappa, bourbon, scotch, calvados, rakia, rum, brandy, whiskey, gin, and rectified ethyl alcohol). The zest of the method is the use of ethanol, present in beverages, as a reference substance for quantitative determination of mentioned components. Checking of precision data, obtained under repeatability conditions and under both repeatability and intermediate precision conditions, and trueness of test results, was carried out according to the ISO 5725–6. The relative difference between calibration coefficients (relative response factors for analyzed volatile compound relative to ethanol), obtained with an interval of 3 weeks, did not exceed 1.1%. Contents of acetaldehyde, methanol, and volatiles in 15 commercial alcoholic beverages analyzed by the developed method varied in the 1.84–677 mg L{−1} of absolute ethanol,3.25–12,394 mg L{−1} of absolute ethanol, and 1.49–4243 mg L{−1} of absolute ethanol intervals, correspondingly.

وصف الملف: application/pdf

URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::8c6bb6fae4f3b78cb1437921226b6ab4
https://doi.org/10.1007/s12161-021-02047-8