دورية أكاديمية
Study on ionic liquid-based ultrasonic-assisted extraction of biphenyl cyclooctene lignans from the fruit of Schisandra chinensis Baill.
العنوان: | Study on ionic liquid-based ultrasonic-assisted extraction of biphenyl cyclooctene lignans from the fruit of Schisandra chinensis Baill. |
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المؤلفون: | Ma CH; Key Laboratory of Forest Plant Ecology, Northeast Forestry University, 150040 Harbin, PR China., Liu TT, Yang L, Zu YG, Wang SY, Zhang RR |
المصدر: | Analytica chimica acta [Anal Chim Acta] 2011 Mar 09; Vol. 689 (1), pp. 110-6. Date of Electronic Publication: 2011 Jan 18. |
نوع المنشور: | Journal Article; Research Support, Non-U.S. Gov't |
اللغة: | English |
بيانات الدورية: | Publisher: Elsevier Country of Publication: Netherlands NLM ID: 0370534 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1873-4324 (Electronic) Linking ISSN: 00032670 NLM ISO Abbreviation: Anal Chim Acta Subsets: MEDLINE |
أسماء مطبوعة: | Publication: Amsterdam : Elsevier Original Publication: Amsterdam. |
مواضيع طبية MeSH: | Cyclooctanes/*isolation & purification , Fruit/*chemistry , Ionic Liquids/*chemistry , Lignans/*isolation & purification , Polycyclic Compounds/*isolation & purification , Schisandra/*chemistry , Solid Phase Extraction/*methods, Chromatography, High Pressure Liquid ; Plant Extracts/chemistry ; Time Factors ; Ultrasonics |
مستخلص: | The ionic liquid-based ultrasonic-assisted extraction (ILUAE) has been successfully applied in extracting four biphenyl cyclooctene lignans from the fruit of Schisandra chinensis Baill. Seventeen different types of ionic liquids with different cations and anions have been investigated. 0.8 M 1-lauryl-3-methylimidazolium bromide ([C12mim]Br) solution was selected as solvent. In addition, the ultrasonic parameters including ultrasonic power, time for ultrasonic treatment and solid-liquid ratio have been optimized by Response Surface Method (RSM). Compared with the conventional solvent extraction, the efficiency of the approach proposed in this work is about 3.5 times as much as that of the conventional solvent extraction method. With the proposed extraction method, the extraction time has been reduced to 30 min, whereas the conventional extraction method requires about 6.0 h. The experimental results presented in this work indicate that the ILUAE is a simple and efficient technique for sample preparation. The proposed method is reproducible. (Crown Copyright © 2011. Published by Elsevier B.V. All rights reserved.) |
المشرفين على المادة: | 0 (Cyclooctanes) 0 (Ionic Liquids) 0 (Lignans) 0 (Plant Extracts) 0 (Polycyclic Compounds) 74XQL5DO3S (schizandrin A) G01BQC0879 (schizandrin) |
تواريخ الأحداث: | Date Created: 20110223 Date Completed: 20110823 Latest Revision: 20171116 |
رمز التحديث: | 20240628 |
DOI: | 10.1016/j.aca.2011.01.012 |
PMID: | 21338765 |
قاعدة البيانات: | MEDLINE |
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