دورية أكاديمية
Challenges and trends for halogen determination by inductively coupled plasma mass spectrometry: A review.
| العنوان: | Challenges and trends for halogen determination by inductively coupled plasma mass spectrometry: A review. |
|---|---|
| المؤلفون: | Flores EMM; Departamento de Química, Universidade Federal de Santa Maria, 97105-900, Santa Maria, RS, Brazil., Mello PA; Departamento de Química, Universidade Federal de Santa Maria, 97105-900, Santa Maria, RS, Brazil., Krzyzaniak SR; Departamento de Química, Universidade Federal de Santa Maria, 97105-900, Santa Maria, RS, Brazil., Cauduro VH; Departamento de Química, Universidade Federal de Santa Maria, 97105-900, Santa Maria, RS, Brazil., Picoloto RS; Departamento de Química, Universidade Federal de Santa Maria, 97105-900, Santa Maria, RS, Brazil. |
| المصدر: | Rapid communications in mass spectrometry : RCM [Rapid Commun Mass Spectrom] 2020 Sep; Vol. 34 Suppl 3, pp. e8727. Date of Electronic Publication: 2020 May 22. |
| نوع المنشور: | Journal Article; Review |
| اللغة: | English |
| بيانات الدورية: | Publisher: John Wiley And Sons Ltd Country of Publication: England NLM ID: 8802365 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1097-0231 (Electronic) Linking ISSN: 09514198 NLM ISO Abbreviation: Rapid Commun Mass Spectrom Subsets: PubMed not MEDLINE; MEDLINE |
| أسماء مطبوعة: | Publication: Chichester : John Wiley And Sons Ltd Original Publication: London, UK : Heyden, c1987- |
| مستخلص: | Rationale: In this review, works published in the past 25 years for fluorine, chlorine, bromine, and iodine determination in several matrices by inductively coupled plasma mass spectrometry (ICP-MS) were covered. Usually, the determination of halogens has been performed by ICP-MS using a previous sample preparation step or, more recently, by direct analysis of solid or liquid samples. Methods: Methods based on combustion, extraction, pyrohydrolysis, sample dilution in organic or aqueous medium, and wet digestion, among others, are discussed. Moreover, the recent applications of methods based on laser ablation (LA) and electrothermal vaporization (ETV) coupled to ICP-MS are discussed. Results: The main challenge for methods using sample preparation has been to obtain a final solution compatible with ICP-MS, as well as to overcome problems related to analyte losses and contamination. Interferences due to the presence of dissolved organic compounds in solution, enhancement or suppression of ionization of analytes, and related matrix effects have been of concern when using ICP-MS. For the determination of halogens by ICP-MS using LA and ETV systems, some limitations related to the difficulty of calibration are pointed out, impairing the widespread use of this approach. Conclusions: A critical view is presented for further halogen determination by ICP-MS, mainly for matrices considered difficult to digest using conventional protocols. (© 2020 John Wiley & Sons, Ltd.) |
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| معلومات مُعتمدة: | 426315/2016-2_Rochele S. Picoloto Conselho Nacional de Desenvolvimento Científico e Tecnológico; INCTBio (Proc. Nr. 573672/2008-3)_Erico M. M. Flores Conselho Nacional de Desenvolvimento Científico e Tecnológico; Finance Code 001 Coordenação de Aperfeiçoamento de Pessoal de Nível Superior |
| تواريخ الأحداث: | Date Created: 20200118 Date Completed: 20200921 Latest Revision: 20200921 |
| رمز التحديث: | 20221213 |
| DOI: | 10.1002/rcm.8727 |
| PMID: | 31950534 |
| قاعدة البيانات: | MEDLINE |
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