دورية أكاديمية
أعرض في EDS

Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil.

التفاصيل البيبلوغرافية
العنوان: Agrochemical Residues in Fish and Bivalves from Sepetiba Bay and Parnaiba River Delta, Brazil.
المؤلفون: Miranda JAT; Biophysics Institute Carlos Chagas Filho, Universidade Federal do Rio de Janeiro (IBCCF-UFRJ), Av. Carlos Chagas Filho, 373, Rio de Janeiro 21941-902, RJ, Brazil., Fogaça FHS; Brazilian Agricultural Research Company, Agroindústria de Alimentos (EMBRAPA), Av. das Américas, nº 29.501, Guaratiba, Rio de Janeiro 23020-470, RJ, Brazil., Cunha SC; Laboratory of Bromatology and Hydrology (LAQV-REQUIMTE), Faculty of Pharmacy, University of Porto, Rua Jorge de Viterbo Ferreira 228, 4050-313 Porto, Portugal., Alonso MB; Biophysics Institute Carlos Chagas Filho, Universidade Federal do Rio de Janeiro (IBCCF-UFRJ), Av. Carlos Chagas Filho, 373, Rio de Janeiro 21941-902, RJ, Brazil., Torres JPM; Biophysics Institute Carlos Chagas Filho, Universidade Federal do Rio de Janeiro (IBCCF-UFRJ), Av. Carlos Chagas Filho, 373, Rio de Janeiro 21941-902, RJ, Brazil., Fernandes JO; Laboratory of Bromatology and Hydrology (LAQV-REQUIMTE), Faculty of Pharmacy, University of Porto, Rua Jorge de Viterbo Ferreira 228, 4050-313 Porto, Portugal.
المصدر: International journal of environmental research and public health [Int J Environ Res Public Health] 2022 Nov 27; Vol. 19 (23). Date of Electronic Publication: 2022 Nov 27.
نوع المنشور: Journal Article; Research Support, Non-U.S. Gov't
اللغة: English
بيانات الدورية: Publisher: MDPI Country of Publication: Switzerland NLM ID: 101238455 Publication Model: Electronic Cited Medium: Internet ISSN: 1660-4601 (Electronic) Linking ISSN: 16604601 NLM ISO Abbreviation: Int J Environ Res Public Health Subsets: MEDLINE
أسماء مطبوعة: Original Publication: Basel : MDPI, c2004-
مواضيع طبية MeSH: Bivalvia*/chemistry , Pesticides*/analysis , Smegmamorpha*, Animals ; Humans ; Tandem Mass Spectrometry/methods ; Bays ; Agrochemicals ; Gas Chromatography-Mass Spectrometry/methods ; Fishes ; Solid Phase Extraction/methods
مستخلص: Accumulation of pesticides has a harmful impact on the environment and human health. The main goal of this work was to develop a method to determine and quantify the residues of thirteen pesticides in edible fish and bivalves such as parati ( Mugil curema ), seabass ( Centropomus ssp.), mullet ( Mugil brasiliensis ), clams ( Anomalocardia brasiliana ) and mussel ( Mytilus galloprovincialis ) collected from Sepetiba Bay and Parnaiba River Delta (Brazil) between 2019 and 2020. Matrix solid-phase dispersion (MSPD) was used for extraction and quantification through gas chromatography coupled to tandem mass spectrometry (GC-MS/MS). The method was validated (linearity, accuracy and precision) for fatty fish ( Salmo salar ), lean fish ( Mugil curema ) and bivalves ( Mytilus edulis ). The survey found linear correlation coefficients (r) equal to or greater than 0.9 for almost all analytes. The relative standard deviations (RSD) of five replicates were less than 20% for almost all analytes at different concentrations in lean fish, fatty fish and bivalves. Most analytes showed satisfactory accuracy. Alachlor herbicide was found in samples of seabass, mussels, clams and parati with levels ranging between 0.55 to 420.39 μg kg -1 dw. Ethion was found in parati (maximum 211.22 μg kg -1 dw), mussels (15.1 μg kg -1 dw) and clams (maximum 44.50 μg kg -1 dw). Alachlor was found in clams (maximum 93.1 μg kg -1 dw), and bifenthrin was found in parati (maximum 43.4 μg kg -1 dw) and clams (maximum 42.21 μg kg -1 dw). The validated method was satisfactory for the determination of eleven pesticides in the fatty fish matrix, and thirteen pesticides in the samples of lean fish and bivalves. The presence of alachlor, ethion and bifenthrin stands out.
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فهرسة مساهمة: Keywords: GC-MS/MS; MSPD; organochlorine; organophosphorus; pyrethroids; seafood
المشرفين على المادة: 0 (Agrochemicals)
0 (Pesticides)
تواريخ الأحداث: Date Created: 20221211 Date Completed: 20221216 Latest Revision: 20240908
رمز التحديث: 20240909
مُعرف محوري في PubMed: PMC9736463
DOI: 10.3390/ijerph192315790
PMID: 36497865
قاعدة البيانات: MEDLINE
الوصف
تدمد:1660-4601
DOI:10.3390/ijerph192315790