دورية أكاديمية
Automatic MDSPE Combined with DART-HRMS for the Rapid Quantitation of 21 Synthetic Cathinones in Urine.
| العنوان: | Automatic MDSPE Combined with DART-HRMS for the Rapid Quantitation of 21 Synthetic Cathinones in Urine. |
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| المؤلفون: | Li Y; China State Institute of Pharmaceutical Industry, State Key Laboratory of New Drug and Pharmaceutical Process, Shanghai 200040, China.; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Lian R; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Sheng Z; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Mao J; Huangpu Branch of Shanghai Public Security Bureau, Shanghai 200010, China., Mao C; Huangpu Branch of Shanghai Public Security Bureau, Shanghai 200010, China., Liang C; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Zhang P; Shanghai Shaanxi Coal Hi-tech Research Institute Co., Ltd., Shanghai 201613, China., Ni C; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Wang R; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China., Zhang Y; Shanghai Key Laboratory of Crime Scene Evidence, Shanghai Institute of Forensic Science, Shanghai 200083, China. |
| المصدر: | Journal of the American Society for Mass Spectrometry [J Am Soc Mass Spectrom] 2024 Jan 03; Vol. 35 (1), pp. 40-49. Date of Electronic Publication: 2023 Dec 18. |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: ACS Publications Country of Publication: United States NLM ID: 9010412 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1879-1123 (Electronic) Linking ISSN: 10440305 NLM ISO Abbreviation: J Am Soc Mass Spectrom Subsets: MEDLINE |
| أسماء مطبوعة: | Publication: 2020- : Washington, DC : ACS Publications Original Publication: New York, NY : Elsevier, c1990- |
| مواضيع طبية MeSH: | Synthetic Cathinone* , Tandem Mass Spectrometry*, Chromatography, Liquid/methods ; Solid Phase Extraction ; Reference Standards |
| مستخلص: | A new, rapid, and automated method for the quantitation of 21 synthetic cathinones in urine was established using magnetic dispersive solid-phase extraction (MDSPE) in combination with direct analysis in real time-high-resolution mass spectrometry (DART-HRMS). Sample preparation and quantitation were verified by liquid chromatography-tandem mass spectrometry (LC-MS/MS). Methcathinone-D3, α-PVP-D8, and proadifen (SKF525A) were used as internal standards. Magnetic HLB extractant and NaH |
| فهرسة مساهمة: | Keywords: direct analysis in real time; high-resolution mass spectrometry; magnetic dispersive solid-phase extraction; rapid quantitation; synthetic cathinones |
| المشرفين على المادة: | 0 (Synthetic Cathinone) |
| تواريخ الأحداث: | Date Created: 20231218 Date Completed: 20240104 Latest Revision: 20240104 |
| رمز التحديث: | 20240104 |
| DOI: | 10.1021/jasms.3c00299 |
| PMID: | 38109269 |
| قاعدة البيانات: | MEDLINE |
Find this article in full text from Springer Verlag. 
Find this issue from the American Chemical Society | تدمد: | 1879-1123 |
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| DOI: | 10.1021/jasms.3c00299 |