دورية أكاديمية
Development and validation of an analytical methodology based on solvent microextraction and UHPLC-MS/MS for determining bisphenols in honeys from different botanical origins.
العنوان: | Development and validation of an analytical methodology based on solvent microextraction and UHPLC-MS/MS for determining bisphenols in honeys from different botanical origins. |
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المؤلفون: | Martín-Gómez B; Analytical Chemistry Group (TESEA), I. U. CINQUIMA, Faculty of Sciences, University of Valladolid, 47011 Valladolid, Spain., Valverde S; Analytical Chemistry Group (TESEA), I. U. CINQUIMA, Faculty of Sciences, University of Valladolid, 47011 Valladolid, Spain., Bernal J; Analytical Chemistry Group (TESEA), I. U. CINQUIMA, Faculty of Sciences, University of Valladolid, 47011 Valladolid, Spain., Ares AM; Analytical Chemistry Group (TESEA), I. U. CINQUIMA, Faculty of Sciences, University of Valladolid, 47011 Valladolid, Spain. Electronic address: ana.maria.ares@uva.es. |
المصدر: | Food chemistry [Food Chem] 2024 Aug 30; Vol. 450, pp. 139358. Date of Electronic Publication: 2024 Apr 15. |
نوع المنشور: | Journal Article; Evaluation Study; Validation Study |
اللغة: | English |
بيانات الدورية: | Publisher: Elsevier Applied Science Publishers Country of Publication: England NLM ID: 7702639 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1873-7072 (Electronic) Linking ISSN: 03088146 NLM ISO Abbreviation: Food Chem Subsets: MEDLINE |
أسماء مطبوعة: | Publication: Barking : Elsevier Applied Science Publishers Original Publication: Barking, Eng., Applied Science Publishers. |
مواضيع طبية MeSH: | Phenols*/analysis , Phenols*/isolation & purification , Tandem Mass Spectrometry* , Honey*/analysis , Benzhydryl Compounds*/analysis , Benzhydryl Compounds*/isolation & purification , Benzhydryl Compounds*/chemistry , Liquid Phase Microextraction*/methods , Food Contamination*/analysis, Chromatography, High Pressure Liquid |
مستخلص: | A new analytical methodology was proposed to determine fourteen bisphenols in honeys from different botanical origins using ultra-high performance liquid chromatography-tandem mass spectrometry. A fast, efficient, environmentally-friendly and simple sample treatment (recoveries between 81% and 116%; matrix effect <20% for all studied compounds except for bisphenol E, F and S) was proposed, which involved a solvent microextraction with acetone and a small volume/amount of 1-hexanol. Chromatographic analysis (< 15 min) was performed in a Kinetex EVO C Competing Interests: Declaration of competing interest The authors of this manuscript declare no conflict of interest. (Copyright © 2024 The Authors. Published by Elsevier Ltd.. All rights reserved.) |
فهرسة مساهمة: | Keywords: Bisphenols; Food safety; Green analytical chemistry; Honey; Method validation; Sample treatment; UHPLC-MS/MS |
المشرفين على المادة: | 0 (Phenols) 0 (Benzhydryl Compounds) MLT3645I99 (bisphenol A) |
تواريخ الأحداث: | Date Created: 20240417 Date Completed: 20240525 Latest Revision: 20240525 |
رمز التحديث: | 20240525 |
DOI: | 10.1016/j.foodchem.2024.139358 |
PMID: | 38631201 |
قاعدة البيانات: | MEDLINE |
تدمد: | 1873-7072 |
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DOI: | 10.1016/j.foodchem.2024.139358 |