دورية أكاديمية
Different spectrophotometric methods applied for the analysis of binary mixture of flucloxacillin and amoxicillin: A comparative study.
| العنوان: | Different spectrophotometric methods applied for the analysis of binary mixture of flucloxacillin and amoxicillin: A comparative study. |
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| المؤلفون: | Attia KA; Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Al-Azhar University, 11751, Nasr City, Cairo, Egypt., Nassar MW; Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Al-Azhar University, 11751, Nasr City, Cairo, Egypt., El-Zeiny MB; Analytical Chemistry Department, Faculty of Pharmacy, Modern University for Technology and Information (MTI), 12582, Al Hadaba Al Wosta, Cairo, Egypt., Serag A; Pharmaceutical Analytical Chemistry Department, Faculty of Pharmacy, Al-Azhar University, 11751, Nasr City, Cairo, Egypt. Electronic address: Ahmedserag777@hotmail.com. |
| المصدر: | Spectrochimica acta. Part A, Molecular and biomolecular spectroscopy [Spectrochim Acta A Mol Biomol Spectrosc] 2016 May 15; Vol. 161, pp. 64-9. Date of Electronic Publication: 2016 Mar 02. |
| نوع المنشور: | Journal Article; Validation Study |
| اللغة: | English |
| بيانات الدورية: | Publisher: Elsevier Country of Publication: England NLM ID: 9602533 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1873-3557 (Electronic) Linking ISSN: 13861425 NLM ISO Abbreviation: Spectrochim Acta A Mol Biomol Spectrosc Subsets: MEDLINE |
| أسماء مطبوعة: | Publication: Original Publication: [Kidlington, Oxford, U.K. ; Tarrytown, NY] : Pergamon, c1994- |
| مواضيع طبية MeSH: | Amoxicillin/*analysis , Anti-Bacterial Agents/*analysis , Floxacillin/*analysis , Spectrophotometry/*methods, Analysis of Variance ; Capsules ; Drug Combinations ; Limit of Detection |
| مستخلص: | Three different spectrophotometric methods were applied for the quantitative analysis of flucloxacillin and amoxicillin in their binary mixture, namely, ratio subtraction, absorbance subtraction and amplitude modulation. A comparative study was done listing the advantages and the disadvantages of each method. All the methods were validated according to the ICH guidelines and the obtained accuracy, precision and repeatability were found to be within the acceptable limits. The selectivity of the proposed methods was tested using laboratory prepared mixtures and assessed by applying the standard addition technique. So, they can be used for the routine analysis of flucloxacillin and amoxicillin in their binary mixtures. (Copyright © 2016 Elsevier B.V. All rights reserved.) |
| فهرسة مساهمة: | Keywords: Absorbance subtraction; Amoxicillin; Amplitude modulation; Flucloxacillin; Ratio subtraction |
| المشرفين على المادة: | 0 (Anti-Bacterial Agents) 0 (Capsules) 0 (Drug Combinations) 43B2M34G2V (Floxacillin) 804826J2HU (Amoxicillin) |
| تواريخ الأحداث: | Date Created: 20160308 Date Completed: 20161213 Latest Revision: 20191210 |
| رمز التحديث: | 20240628 |
| DOI: | 10.1016/j.saa.2016.02.028 |
| PMID: | 26950503 |
| قاعدة البيانات: | MEDLINE |
Full Text Finder | تدمد: | 1873-3557 |
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| DOI: | 10.1016/j.saa.2016.02.028 |