دورية أكاديمية
Simple synthesis of a clew-like tungsten carbide nanocomposite decorated with gold nanoparticles for the ultrasensitive detection of tert-butylhydroquinone.
العنوان: | Simple synthesis of a clew-like tungsten carbide nanocomposite decorated with gold nanoparticles for the ultrasensitive detection of tert-butylhydroquinone. |
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المؤلفون: | Ezhil Vilian AT; Department of Energy and Materials Engineering, Dongguk University-Seoul, Seoul 100-715, Republic of Korea., Umapathi R; Department of Biological Engineering, Inha University, Incheon 22212, Republic of Korea., Hwang SK; Department of Biological Engineering, Inha University, Incheon 22212, Republic of Korea., Lee MJ; Department of Biological Engineering, Inha University, Incheon 22212, Republic of Korea., Huh YS; Department of Biological Engineering, Inha University, Incheon 22212, Republic of Korea. Electronic address: yunsuk.huh@inha.ac.kr., Han YK; Department of Energy and Materials Engineering, Dongguk University-Seoul, Seoul 100-715, Republic of Korea. Electronic address: ykenergy@dongguk.edu. |
المصدر: | Food chemistry [Food Chem] 2021 Jun 30; Vol. 348, pp. 128936. Date of Electronic Publication: 2020 Dec 24. |
نوع المنشور: | Journal Article |
اللغة: | English |
بيانات الدورية: | Publisher: Elsevier Applied Science Publishers Country of Publication: England NLM ID: 7702639 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1873-7072 (Electronic) Linking ISSN: 03088146 NLM ISO Abbreviation: Food Chem Subsets: MEDLINE |
أسماء مطبوعة: | Publication: Barking : Elsevier Applied Science Publishers Original Publication: Barking, Eng., Applied Science Publishers. |
مواضيع طبية MeSH: | Limit of Detection* , Nanotechnology*, Gold/*chemistry , Hydroquinones/*analysis , Metal Nanoparticles/*chemistry , Nanocomposites/*chemistry , Tungsten Compounds/*chemistry, Carbon/chemistry ; Chemistry Techniques, Synthetic ; Electrodes ; Humans ; Oxidation-Reduction |
مستخلص: | The excessive use of food additives in manufactured food products negatively affects their quality and potentially impacts human health. In the present study, a composite consisting of gold nanoparticles decorated on tungsten carbide (AuNP-WC) was successfully fabricated using a facile and cost-effective ultrasonication technique. Compared to a bare glassy carbon electrode (GCE), AuNP-GCE, and WC-GCE, the AuNP-WC-GCE demonstrated excellent sensing performance for tert-butylhydroquinone (TBHQ) when used as an electrocatalyst in 0.05 M phosphate buffer solution (PBS), with a low working potential and a high peak current. In particular, the composite was able to detect the oxidation of TBHQ within a linear concentration range of 5 to 75 nM, with an extremely low detection limit of 0.20 nM. The practicability of the sensor was also assessed in the analysis of TBHQ in real samples of soybean oil, blended oil, and red wine, with satisfactory recovery rates obtained. (Copyright © 2020 Elsevier Ltd. All rights reserved.) |
فهرسة مساهمة: | Keywords: Electrochemical detection; Gold nanoparticles; Square wave voltammetry; Tert-butylhydroquinone; Tungsten carbide |
المشرفين على المادة: | 0 (Hydroquinones) 0 (Tungsten Compounds) 11130-73-7 (tungsten carbide) 7440-44-0 (Carbon) 7440-57-5 (Gold) C12674942B (2-tert-butylhydroquinone) |
تواريخ الأحداث: | Date Created: 20210128 Date Completed: 20210322 Latest Revision: 20210322 |
رمز التحديث: | 20231215 |
DOI: | 10.1016/j.foodchem.2020.128936 |
PMID: | 33508604 |
قاعدة البيانات: | MEDLINE |
تدمد: | 1873-7072 |
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DOI: | 10.1016/j.foodchem.2020.128936 |