دورية أكاديمية
[Simultaneous determination of 40 plant growth regulators, fungicides, insecticides, and antibiotics in bean sprouts by QuEChERS-high performance liquid chromatography-tandem mass spectrometry].
العنوان: | [Simultaneous determination of 40 plant growth regulators, fungicides, insecticides, and antibiotics in bean sprouts by QuEChERS-high performance liquid chromatography-tandem mass spectrometry]. |
---|---|
المؤلفون: | Feng J; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Jiang H; Food and Drug Inspection Center of Handan City, Handan 056004, China., Wang J; College of Materials Science and Engineering, Hebei University of Engineering, Handan 056038, China., Jing Z; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Zhang F; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Tan T; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., He F; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Jiang L; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Li H; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Chang S; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China., Li T; College of Life Science and Food Engineering, Hebei University of Engineering, Handan 056038, China. |
المصدر: | Se pu = Chinese journal of chromatography [Se Pu] 2022 Sep; Vol. 40 (9), pp. 843-853. |
نوع المنشور: | Journal Article |
اللغة: | Chinese |
بيانات الدورية: | Publisher: Hua xue za zhi she Country of Publication: China NLM ID: 9424804 Publication Model: Print Cited Medium: Internet ISSN: 1872-2059 (Electronic) Linking ISSN: 10008713 NLM ISO Abbreviation: Se Pu Subsets: MEDLINE |
أسماء مطبوعة: | Original Publication: Dalian Shi : Hua xue za zhi she |
مواضيع طبية MeSH: | Chlorpyrifos* , Fungicides, Industrial*/analysis , Insecticides*/analysis, 2,4-Dichlorophenoxyacetic Acid/analogs & derivatives ; 2,4-Dichlorophenoxyacetic Acid/analysis ; Acetonitriles ; Adenine ; Ammonia ; Anti-Bacterial Agents ; Benzimidazoles ; Benzyl Compounds ; Carbamates ; Chloramphenicol/analysis ; Chlormequat ; Chromatography, High Pressure Liquid ; Ciprofloxacin ; Dimetridazole ; Enoxacin ; Enrofloxacin ; Gibberellins ; Levofloxacin ; Methanol ; Methomyl ; Metronidazole ; Norfloxacin ; Pefloxacin ; Plant Growth Regulators/analysis ; Purines ; Ronidazole ; Solvents ; Tandem Mass Spectrometry ; Thiabendazole |
مستخلص: | Chromatography combined with mass spectrometry is the most commonly used detection technology, and it offers the advantages of high sensitivity and high selectivity. The quick, easy, inexpensive, effective, rugged, and safe (QuEChERS) method is low-cost, effective, and time efficient. The application of the QuEChERS has now been extended to the analysis of contaminants in food samples. The aim of the study was to identify different concentration levels of multiple harmful drug residues in bean sprouts. In this study, QuEChERS coupled with high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS) was established for the simultaneous determination of 40 plant growth regulators, fungicides, insecticides, and antibiotics in bean sprouts. In the HPLC-MS/MS experiment, gibberellic acid, 4-fluorophenoxyacetic acid, chloramphenicol, N 6-( δ 2-isopentenyl)-adenine, 6-benzylaminopurine, 4-chlorophenoxyacetic acid, and 2,4-dichlorophenoxyacetic acid (2,4-D) were analyzed by MS/MS with negative electrospray ionization (ESI - ). The other 33 target analytes (chlormequat, ronidazole, metronidazole, pymetrozine, dimetridazole, methomyl, carbendazim, enoxacin, levofloxacin, pefloxacin mesylate, norfloxacin, ciprofloxacin, enrofloxacin, thiabendazole, lomefloxacin, chlorpyrifos, sarafloxacin, imidacloprid, etc.) were analyzed by MS/MS with positive electrospray ionization (ESI + ). Sensitive MS conditions were realized by optimizing the instrumental parameters such as the desolvent temperature, collision energy, spraying needle position, precursor ions, and product ions. Then, the optimal pretreatment method was determined by comparing the recovery rates of the 40 drugs obtained with different extraction solvents (methanol, acetonitrile, acetonitrile containing 0.1% ammonia, acetonitrile with 1% acetic acid), different extraction methods (ultrasonic extraction, shaking extraction), and purification with primary secondary amine (PSA) and C |
References: | Food Chem. 2020 Aug 30;322:126766. (PMID: 32305873) Food Chem. 2020 May 1;311:125999. (PMID: 31864185) Se Pu. 2018 Jul 8;36(7):659-664. (PMID: 30136538) Se Pu. 2019 Sep 8;37(9):946-954. (PMID: 31642298) Se Pu. 2021 Aug;39(8):878-888. (PMID: 34212588) Food Chem. 2016 Oct 1;208:239-44. (PMID: 27132845) Food Chem. 2017 Feb 15;217:311-319. (PMID: 27664639) J Chromatogr A. 2018 May 11;1549:14-24. (PMID: 29588097) Food Chem. 2020 Feb 15;306:125455. (PMID: 31629968) Se Pu. 2021 Apr 8;39(4):406-414. (PMID: 34227761) |
فهرسة مساهمة: | Keywords: QuEChERS; antibiotics; bean sprout; fungicides; high performance liquid chromatography-tandem mass spectrometry (HPLC-MS/MS); insecticide; plant growth regulators |
المشرفين على المادة: | 0 (Acetonitriles) 0 (Anti-Bacterial Agents) 0 (Benzimidazoles) 0 (Benzyl Compounds) 0 (Carbamates) 0 (Fungicides, Industrial) 0 (Gibberellins) 0 (Insecticides) 0 (Plant Growth Regulators) 0 (Purines) 0 (Solvents) 140QMO216E (Metronidazole) 1NQ08HN02S (Methomyl) 2577AQ9262 (2,4-Dichlorophenoxyacetic Acid) 2H52Z9F2Q5 (Pefloxacin) 325OGW249P (Enoxacin) 3DX3XEK1BN (Enrofloxacin) 4EMM3U5P3K (4-chlorophenoxyacetic acid) 5E8K9I0O4U (Ciprofloxacin) 66974FR9Q1 (Chloramphenicol) 6GNT3Y5LMF (Levofloxacin) 7664-41-7 (Ammonia) 8SUZ1123XX (Chlormequat) BU0A7MWB6L (gibberellic acid) E01R4M1063 (Ronidazole) H75J14AA89 (carbendazim) JAC85A2161 (Adenine) JCS58I644W (Chlorpyrifos) K59P7XNB8X (Dimetridazole) KXG6A989PS (benzylaminopurine) N0F8P22L1P (Norfloxacin) N1Q45E87DT (Thiabendazole) Y4S76JWI15 (Methanol) |
تواريخ الأحداث: | Date Created: 20220926 Date Completed: 20220928 Latest Revision: 20221001 |
رمز التحديث: | 20231215 |
مُعرف محوري في PubMed: | PMC9520376 |
DOI: | 10.3724/SP.J.1123.2021.12028 |
PMID: | 36156631 |
قاعدة البيانات: | MEDLINE |
تدمد: | 1872-2059 |
---|---|
DOI: | 10.3724/SP.J.1123.2021.12028 |