دورية أكاديمية
New Analytical Strategy for Bioaccessibility Evaluation of Bromine and Iodine from Edible Seaweeds.
| العنوان: | New Analytical Strategy for Bioaccessibility Evaluation of Bromine and Iodine from Edible Seaweeds. |
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| المؤلفون: | Scaglioni PT; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil., Balbinot FP; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil., Rondan FS; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil., Novo DLR; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil., Silva AA; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil., Mesko MF; Centro de Ciências Químicas, Farmacêuticas e de Alimentos, Universidade Federal de Pelotas, 96160-000 Capão do Leão, RS, Brazil. |
| المصدر: | Journal of agricultural and food chemistry [J Agric Food Chem] 2023 Mar 27. Date of Electronic Publication: 2023 Mar 27. |
| Publication Model: | Ahead of Print |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: American Chemical Society Country of Publication: United States NLM ID: 0374755 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1520-5118 (Electronic) Linking ISSN: 00218561 NLM ISO Abbreviation: J Agric Food Chem Subsets: MEDLINE |
| أسماء مطبوعة: | Original Publication: Washington, American Chemical Society. |
| مستخلص: | A strategy for determining the bioaccessibility of bromine and iodine from edible seaweeds was proposed for the first time using microwave-induced combustion (MIC) and ion chromatography coupled to mass spectrometry (IC-MS) after in vitro digestion. The concentrations of bromine and iodine in edible seaweeds using the proposed methods (MIC and IC-MS) were not statistically different from those using MIC and inductively coupled plasma mass spectrometry ( p > 0.05). Trueness was assessed by recovery experiments (101-110%, relative standard deviation <10%). Following an in vitro digestion protocol, MIC was proposed as sample preparation for bioaccessible and residual fractions. Using this strategy, the mass balance totaled from 97 to 111%. No statistical difference ( p > 0.05) was observed between the total concentration of bromine or iodine and their concentration in bioaccessible and residual fractions for three edible seaweed species, indicating full analyte quantification in the fractions. |
| فهرسة مساهمة: | Keywords: food nutrition; halogens; in vitro digestion; ion chromatography coupled to mass spectrometry; microwave-induced combustion; sample preparation |
| تواريخ الأحداث: | Date Created: 20230327 Latest Revision: 20230327 |
| رمز التحديث: | 20231215 |
| DOI: | 10.1021/acs.jafc.2c08541 |
| PMID: | 36972393 |
| قاعدة البيانات: | MEDLINE |
Find this issue from the American Chemical Society | تدمد: | 1520-5118 |
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| DOI: | 10.1021/acs.jafc.2c08541 |