دورية أكاديمية
Application of physical vapor deposition technology for practical utilization of nano-size copper oxide for lead uptake from solution: kinetics, equilibrium, and recycling studies.
| العنوان: | Application of physical vapor deposition technology for practical utilization of nano-size copper oxide for lead uptake from solution: kinetics, equilibrium, and recycling studies. |
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| المؤلفون: | Abdelghani JI; Faculty of Science, Department of Chemistry, The Hashemite University, P.O. Box 150459, Al-Zarqa, 13115, Jordan. j.abdelghani@hu.edu.jo., El-Sheikh AH; Faculty of Science, Department of Chemistry, The Hashemite University, P.O. Box 150459, Al-Zarqa, 13115, Jordan., Al-Hashimi NN; Faculty of Pharmaceutical Sciences, Department of Pharmaceutical Chemistry, The Hashemite University, P.O. Box 330127, Al-Zarqa, 13133, Jordan. |
| المصدر: | Environmental science and pollution research international [Environ Sci Pollut Res Int] 2023 Apr; Vol. 30 (20), pp. 58783-58795. Date of Electronic Publication: 2023 Mar 30. |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: Springer Country of Publication: Germany NLM ID: 9441769 Publication Model: Print-Electronic Cited Medium: Internet ISSN: 1614-7499 (Electronic) Linking ISSN: 09441344 NLM ISO Abbreviation: Environ Sci Pollut Res Int Subsets: MEDLINE |
| أسماء مطبوعة: | Publication: <2013->: Berlin : Springer Original Publication: Landsberg, Germany : Ecomed |
| مواضيع طبية MeSH: | Copper*/chemistry , Water Pollutants, Chemical*/chemistry, Lead ; Kinetics ; Oxides/chemistry ; Adsorption ; Hydrogen-Ion Concentration |
| مستخلص: | For the first time, copper oxide-coated glass beads (CuO-GBs) were fabricated using physical vapor deposition (PVD) technology for sequestrating Pb 2+ ions from solution is addressed. Compared to other coating procedures, PVD offered high-stability uniform CuO nano-layers attached with 3.0-mm glass beads. Heating of copper oxide-coated glass beads after deposition was rather necessary to achieve the best stability of the nano-adsorbent. Detection of nano-size copper oxide on the beads was made by FTIR (intense peak at 655 cm -1 for CuO bond stretching) and XRF (Cu peak at 8.0 keV). Scanning electron micrographs taken at high magnification power indicated the presence of CuO in nano-range deposited over glass beads. The maximum deposited amount of CuO on the beads was 1.1% and accomplished at the following operational conditions: internal pressure 10 -5 mmHg, Ar flow rate 8.0 mL/min, voltage 84 V, pre-sputtering time 20 s, total sputtering time 10.0 min, and post-heating temperature 150 °C for 3 h. A univariate analysis indicated that the optimum Pb 2+ uptake by CuO-GBs from solution was achieved at pH 7.0-8.0, 7 beads/50 mL, 120-min contact time, and 15-mg/L initial concentration. Kinetic data for Pb 2+ uptake was best presented by a pseudo-second-order model with a relative prediction error of 3.2 and 5.1% for GBs and CuO-GBs, respectively. On the other hand, Pb 2+ equilibrium isotherms at 25 °C were fairly presented by the Langmuir model, and the predicted saturation values were 5.48 and 15.69 mg/g for GBs and CuO-GBs, respectively. CuO and CuO-GBs had similar Pb 2+ saturation values (~ 16 mg/g), although the latter demonstrated 4 times faster kinetic, thanks to fixation CuO on glass beads. Moreover, the chemical stability of copper oxide-coated glass beads was tested under different conditions. Recycling of copper oxide-coated glass beads was also investigated, and 90% of the surface was recovered using 0.01-M HNO (© 2023. The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature.) |
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| فهرسة مساهمة: | Keywords: Adsorption; Nano-size CuO; Physical vapor deposition; Pre-concentration; Recycling |
| المشرفين على المادة: | V1XJQ704R4 (cupric oxide) T8BEA5064F (cuprous oxide) 789U1901C5 (Copper) 2P299V784P (Lead) 0 (Oxides) 0 (Water Pollutants, Chemical) |
| تواريخ الأحداث: | Date Created: 20230330 Date Completed: 20230510 Latest Revision: 20230510 |
| رمز التحديث: | 20240628 |
| DOI: | 10.1007/s11356-023-26591-4 |
| PMID: | 36997786 |
| قاعدة البيانات: | MEDLINE |
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Full Text Finder | تدمد: | 1614-7499 |
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| DOI: | 10.1007/s11356-023-26591-4 |