دورية أكاديمية
Rice powder template for hausmannite Mn3O4 nanoparticles and its application to aqueous zinc ion battery.
| العنوان: | Rice powder template for hausmannite Mn3O4 nanoparticles and its application to aqueous zinc ion battery. |
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| المؤلفون: | Tonu NT; Department of Chemistry, Khulna University of Engineering & Technology, Khulna, Bangladesh.; Chemistry Discipline, Khulna University, Khulna, Bangladesh., Ahamed P; Department of Chemistry, Khulna University of Engineering & Technology, Khulna, Bangladesh., Yousuf MA; Department of Chemistry, Khulna University of Engineering & Technology, Khulna, Bangladesh. |
| المصدر: | PloS one [PLoS One] 2024 Jun 17; Vol. 19 (6), pp. e0305611. Date of Electronic Publication: 2024 Jun 17 (Print Publication: 2024). |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: Public Library of Science Country of Publication: United States NLM ID: 101285081 Publication Model: eCollection Cited Medium: Internet ISSN: 1932-6203 (Electronic) Linking ISSN: 19326203 NLM ISO Abbreviation: PLoS One Subsets: MEDLINE |
| أسماء مطبوعة: | Original Publication: San Francisco, CA : Public Library of Science |
| مواضيع طبية MeSH: | Oryza*/chemistry , Manganese Compounds*/chemistry , Electric Power Supplies* , Zinc*/chemistry , Oxides*/chemistry , Powders* , Nanoparticles*/chemistry, X-Ray Diffraction ; Spectroscopy, Fourier Transform Infrared |
| مستخلص: | In this study, a simple calcination route was adopted to prepare hausmannite Mn3O4 nanoparticles using rice powder as soft bio-template. Prepared Mn3O4 was characterized by Fourier Transform Infra-Red Spectroscopy (FTIR), Field Emission Scanning Electron Microscopy (FESEM), Energy Dispersive X-ray microanalysis (EDX), Powder X-Ray Diffraction (XRD), Transmission Electron Microscopy (TEM), Brunauer-Emmett-Teller (BET) and Solid state UV-Vis spectroscopic techniques. Mn-O stretching in tetrahedral site was confirmed by FTIR and Raman spectra. % of Mn and O content supported Mn3O4 formation. The crystallinity and grain size was found to be 68.76% and 16.43 nm, respectively; tetragonal crystal system was also cleared by XRD. TEM clarified the planes of crystal formed which supported the XRD results and BET demonstrated mesoporous nature of prepared Mn3O4 having low pore volume. Low optical band gap of 3.24 eV of prepared Mn3O4 nanoparticles indicated semiconductor property and was used as cathode material to fabricate CR-2032 coin cell of Aqueous Rechargeable Zinc Ion Battery (ARZIB). A reversible cyclic voltammogram (CV) showed good zinc ion storage performance. Low cell resistance was confirmed by Electrochemical Impedance Spectroscopy (EIS). The coin cell delivered high specific discharge capacity of 240.75 mAhg-1 at 0.1 Ag-1 current density. The coulombic efficiency was found to be 99.98%. It also delivered excellent capacity retention 94.45% and 64.81% after 300 and 1000 charge-discharge cycles, respectively. This work offers a facile and cost effective approach for preparing cathode material of ARZIBs. Competing Interests: The authors have declared that no competing interests exist. (Copyright: © 2024 Tonu et al. This is an open access article distributed under the terms of the Creative Commons Attribution License, which permits unrestricted use, distribution, and reproduction in any medium, provided the original author and source are credited.) |
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| المشرفين على المادة: | 0 (Manganese Compounds) J41CSQ7QDS (Zinc) 0 (Oxides) 64J2OA7MH3 (manganese oxide) 0 (Powders) |
| تواريخ الأحداث: | Date Created: 20240617 Date Completed: 20240617 Latest Revision: 20240619 |
| رمز التحديث: | 20240619 |
| مُعرف محوري في PubMed: | PMC11182549 |
| DOI: | 10.1371/journal.pone.0305611 |
| PMID: | 38885268 |
| قاعدة البيانات: | MEDLINE |
Full Text Finder | تدمد: | 1932-6203 |
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| DOI: | 10.1371/journal.pone.0305611 |