دورية أكاديمية
Utilizing two different sustainable and green spectrophotometric approaches using derivative ratio spectra for the determination of a ternary severely overlapped mixture: application to veterinary formulation.
| العنوان: | Utilizing two different sustainable and green spectrophotometric approaches using derivative ratio spectra for the determination of a ternary severely overlapped mixture: application to veterinary formulation. |
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| المؤلفون: | Abdullatif HA; Pharmaceutical Chemistry Department, Faculty of Pharmacy, Ahram Canadian University, Cairo, Egypt. hanoood7@hotmail.com., Abdelkawy M; Analytical Chemistry Department, Faculty of Pharmacy, Cairo University, Giza, Egypt. dr.mohabdelkawy@hotmail.com., Kamal M; Pharmaceutical Chemistry Department, Faculty of Pharmacy, Ahram Canadian University, Cairo, Egypt., Fahmy NM; Pharmaceutical Chemistry Department, Faculty of Pharmacy, Ahram Canadian University, Cairo, Egypt. |
| المصدر: | BMC chemistry [BMC Chem] 2024 Jun 26; Vol. 18 (1), pp. 118. Date of Electronic Publication: 2024 Jun 26. |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: Springer Nature Country of Publication: Switzerland NLM ID: 101741142 Publication Model: Electronic Cited Medium: Internet ISSN: 2661-801X (Electronic) Linking ISSN: 2661801X NLM ISO Abbreviation: BMC Chem Subsets: PubMed not MEDLINE |
| أسماء مطبوعة: | Original Publication: Cham, Switzerland : Springer Nature, [2019]- |
| مستخلص: | Mathematical manipulation technique has proven to be a very powerful tool for efficient processing and handling of highly overlapped spectra. This work introduced two green and sustainable approaches for the successful recovery of the ternary mixture, Tylosin tartarate (TYL), Sulfadimdine (SLD), and Trimethoprim (TRI). The approaches were constructed using three different methods, derivative ratio spectrum zero-crossing method (DRSZ), double divisor ratio spectra derivative method (DDRD), and factorized derivative ratio method coupled with spectrum subtraction (FDRM-SS). The two approaches succeeded in recovering the three drugs (Linearity range achieved were 0.5-5 µg/mL for TYL, 0.3-1.3 µg/mL for SLD, and 0.3-5 µg/mL for TRI), giving convenient standard deviations and satisfactory recovery percentages. The recommended methods have been verified in accordance with (ICH) guidelines. When the results were statistically compared to the official methods, no significant difference was found. Both AGREE-Analytical GREEnness Metric Approach and Software, and White Analytical Chemistry (WAC) RGB model gave scores of 0.93 and 97.2%, respectively, which proved that the approaches were eco-friendly and abiding by the sustainability principles. (© 2024. The Author(s).) |
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| فهرسة مساهمة: | Keywords: Analytical GREEnness Metric Approach and Software; Sulfadmidine; Sustainable; Ternary severely overlapped; Trimethoprim; Tylosin; Veterinary; White analytical chemistry |
| تواريخ الأحداث: | Date Created: 20240626 Latest Revision: 20240629 |
| رمز التحديث: | 20240629 |
| مُعرف محوري في PubMed: | PMC11209959 |
| DOI: | 10.1186/s13065-024-01220-4 |
| PMID: | 38926795 |
| قاعدة البيانات: | MEDLINE |
Find this article in full text from Springer Verlag. 
Full Text Finder | تدمد: | 2661-801X |
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| DOI: | 10.1186/s13065-024-01220-4 |