دورية أكاديمية
Determination of succinonitrile in horse urine by gas chromatography-nitrogen-phosphorus detector and gas chromatography-mass spectrometry.
| العنوان: | Determination of succinonitrile in horse urine by gas chromatography-nitrogen-phosphorus detector and gas chromatography-mass spectrometry. |
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| المؤلفون: | Pedroso RC; Faculty of Pharmaceutical Sciences, University of São Paulo, Brazil., Salvadori MC, Andraus MH, Lopez NM |
| المصدر: | The Analyst [Analyst] 1994 Dec; Vol. 119 (12), pp. 2697-9. |
| نوع المنشور: | Journal Article |
| اللغة: | English |
| بيانات الدورية: | Publisher: Royal Society of Chemistry Country of Publication: England NLM ID: 0372652 Publication Model: Print Cited Medium: Print ISSN: 0003-2654 (Print) Linking ISSN: 00032654 NLM ISO Abbreviation: Analyst Subsets: MEDLINE |
| أسماء مطبوعة: | Publication: Cambridge : Royal Society of Chemistry Original Publication: London : Chemical Society |
| مواضيع طبية MeSH: | Horses/*urine , Nitriles/*urine, Animals ; Chromatography, Gas/methods ; Female ; Gas Chromatography-Mass Spectrometry/methods ; Mass Screening/veterinary ; Nitriles/isolation & purification |
| مستخلص: | A chromatographic method was developed to detect and confirm the presence of succinonitrile (SDN) in horse urine samples, for antidoping control. The urine samples (5 ml) were extracted with diethyl ether and screened by gas chromatography-nitrogen-phosphorus detector and the confirmation of the drug's presence was accomplished by using gas chromatography-mass selective detection. The recovery of extraction was 78 and 81% for 1.0 and 2.0 micrograms ml-1 (relative standard deviation, < 10%), respectively. Urine samples collected after the administration of Energisan were positive for SDN (1-30 h) in all samples analysed. |
| المشرفين على المادة: | 0 (Nitriles) 1R479O92DO (succinonitrile) |
| تواريخ الأحداث: | Date Created: 19941201 Date Completed: 19950331 Latest Revision: 20190821 |
| رمز التحديث: | 20221213 |
| DOI: | 10.1039/an9941902697 |
| PMID: | 7879879 |
| قاعدة البيانات: | MEDLINE |
| تدمد: | 0003-2654 |
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| DOI: | 10.1039/an9941902697 |