التفاصيل البيبلوغرافية
| العنوان: |
Ultrasound-based surface sampling in immersion for mass spectrometry. |
| المؤلفون: |
Sillanpää, Tom, Hyvönen, Jere, Mäkinen, Joni, Holmström, Axi, Pudas, Topi, Lassila, Petri, Lepistö, Riikka, Kuronen, Antti, Kotiaho, Tapio, Hæggström, Edward, Salmi, Ari |
| المصدر: |
Journal of Applied Physics; 9/14/2023, Vol. 134 Issue 10, p1-13, 13p |
| مصطلحات موضوعية: |
HIGH-intensity focused ultrasound, MASS spectrometry, ELECTROSPRAY ionization mass spectrometry, IMMERSION in liquids, ANALYTICAL chemistry |
| مستخلص: |
We present a surface sampling method for the chemical analysis of liquid-immersed solid samples. Liquid immersion allows samples to be kept in a hydrated state. We employed cavitation generated by high-intensity focused ultrasound for localized material removal. The appropriate transducer–sample distance was determined using the actuating ultrasound transducer prior to sampling, allowing sonication in focus despite surface height variation. We demonstrate the proposed surface sampling method on water-submerged glass cover slides painted with permanent markers, achieving sampling with tunable spot size down to 500 μ m. The removed and collected material was transferred for chemical analysis by electrospray ionization mass spectrometry, which showed mass peaks characteristic to the permanent markers. [ABSTRACT FROM AUTHOR] |
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| قاعدة البيانات: |
Complementary Index |
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