Monitoring solid phase reactions with ion-selective electrode

التفاصيل البيبلوغرافية
العنوان: Monitoring solid phase reactions with ion-selective electrode
المؤلفون: Pátek, Marcel, Bildstein, Sylvia, Flegelová, Zuzana
المصدر: Tetrahedron Letters; January 1998, Vol. 39 Issue: 8 p753-756, 4p
مستخلص: A noninvasive method for monitoring and quantitative determination of basic functionalities (pK hb+>7) on solid support is described and its usefulness is demonstrated with practical examples. The method is based on quantitative protonation of the basic moieties on solid support with perchloric acid, followed by release of perchlorate anions by base and their concomitant potentiometric determination using an ion-selective electrode.
قاعدة البيانات: Supplemental Index
الوصف
تدمد:00404039
DOI:10.1016/S0040-4039(97)10617-7