Pesticide residues analysis in wine by liquid chromatography–tandem mass spectrometry and using ethyl acetate extraction method: validation and pilot survey in real samples
| العنوان: | Pesticide residues analysis in wine by liquid chromatography–tandem mass spectrometry and using ethyl acetate extraction method: validation and pilot survey in real samples |
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| المؤلفون: | Panayiota Hadjiloizou, Popi Kanari, Despo Louca Christodoulou, Panayiotis Constantinou |
| المصدر: | Journal of Wine Research. 26:81-98 |
| بيانات النشر: | Informa UK Limited, 2015. |
| سنة النشر: | 2015 |
| مصطلحات موضوعية: | Wine, chemistry.chemical_compound, Chromatography, Pesticide residue, Chemistry, Liquid chromatography–mass spectrometry, Extraction (chemistry), Ethyl acetate, Pilot survey, Sample preparation, Horticulture, Pesticide, Food Science |
| الوصف: | This paper presents a cost-effective and validated method for the determination of 172 pesticide residues monitored during a survey study on 27 commercially available Cypriot wines (red/white, dry/sweet). Sample preparation involved ethyl acetate extraction of pesticides from wines. For the validation of the method, blank samples were spiked with a solution of 172 pesticides (such as insecticides, fungicides, herbicides) at three levels such as 0.01, 0.05 and 0.1 mg/kg. The samples were analyzed by LC-MS/MS (liquid chromatography tandem mass spectrometry). The validation study was in accordance with the DG SANCO (Directorate-General for Health and Consumers) guidelines [Document No. SANCO/12495/2012. Method validation and quality control procedures for pesticide residues analysis in food and feed]. The scope of validation included recovery, linearity, limits of quantification and precision. Recoveries of the majority of compounds were found to be in the range of 70–120% and were characterized by precision... |
| تدمد: | 1469-9672 0957-1264 |
| URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_________::06533d2f61381c3cb7002d6079bd1a03 https://doi.org/10.1080/09571264.2015.1022255 |
| رقم الأكسشن: | edsair.doi...........06533d2f61381c3cb7002d6079bd1a03 |
| قاعدة البيانات: | OpenAIRE |
PDF full text from Publisher | تدمد: | 14699672 09571264 |
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