Pesticide residues analysis in honey using ethyl acetate extraction method: validation and pilot survey in real samples
| العنوان: | Pesticide residues analysis in honey using ethyl acetate extraction method: validation and pilot survey in real samples |
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| المؤلفون: | Koula Kika, Olympiada Kourouzidou, Panayiota Hadjiloizou, Panayiotis Constantinou, Despo Louca Christodoulou, Maria Constantinou, Popi Kanari |
| المصدر: | International Journal of Environmental Analytical Chemistry. 95:894-910 |
| بيانات النشر: | Informa UK Limited, 2015. |
| سنة النشر: | 2015 |
| مصطلحات موضوعية: | Chromatography, Pesticide residue, Chemistry, Health, Toxicology and Mutagenesis, Extraction (chemistry), Public Health, Environmental and Occupational Health, Ethyl acetate, Soil Science, Pesticide, Mass spectrometry, Tandem mass spectrometry, Pollution, Analytical Chemistry, chemistry.chemical_compound, Electron capture detector, Environmental Chemistry, Gas chromatography, Waste Management and Disposal, Water Science and Technology |
| الوصف: | This paper presents a cost-effective and validated multi residue confirmatory method for the determination of 167 chemically different pesticides and a survey study on Cyprus honey samples. This method uses ethyl acetate for the extraction of pesticides from honey and the determination is performed with liquid chromatography (LC) coupled to mass spectrometry (MS) operating in tandem mode (MS/MS) and with GC–ECD (gas chromatography with electron capture detector) analysis. The LC-MS/MS analytical system is especially important in the analysis of polar and non-volatile pesticides. For the validation of the method, blank honey samples were spiked with 146 pesticides (organophosphorous, carbamates, triazoles, amides, neonicodinoids, strobilurines, phenylureas, bendimidazoles and others) for the LC-MS/MS analysis at three levels: 0.01, 0.05 and 0.1 mg kg−1 and with 21 pesticides for the GC-ECD analysis at two levels: 0.01 and 0.05 mg kg−1for organochlorines and 0.05 and 0.2 mg kg−1for the pyrethroids. As blank... |
| تدمد: | 1029-0397 0306-7319 |
| URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_________::4fe015f0af4c66b35b86f27299ddcedc https://doi.org/10.1080/03067319.2015.1070408 |
| رقم الأكسشن: | edsair.doi...........4fe015f0af4c66b35b86f27299ddcedc |
| قاعدة البيانات: | OpenAIRE |
PDF full text from Publisher | تدمد: | 10290397 03067319 |
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