Electrochemical synthesis of sulfonamides in a graphite powder macroelectrode
| العنوان: | Electrochemical synthesis of sulfonamides in a graphite powder macroelectrode |
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| المؤلفون: | Danilo Galdino, Paulo H. Menezes, Marcelo Navarro, Dmistocles A. Vicente |
| المصدر: | Green Chemistry. 22:5262-5266 |
| بيانات النشر: | Royal Society of Chemistry (RSC), 2020. |
| سنة النشر: | 2020 |
| مصطلحات موضوعية: | chemistry.chemical_classification, Primary (chemistry), 010405 organic chemistry, Chemistry, Radical, Inorganic chemistry, Aqueous electrolyte, Sulfinic acid, 010402 general chemistry, Electrochemistry, 01 natural sciences, Pollution, 0104 chemical sciences, Sodium salt, Environmental Chemistry, Graphite |
| الوصف: | The electrochemical generation of sulfinyl radicals from commercially available and non-expensive sodium salts of sulfinic acids is described. Electrooxidation reactions were carried out in a graphite powder macroelectrode using an aqueous electrolyte and cavity cell. Further reaction with primary or secondary amines gave the corresponding sulfonamides, a unit present in several biologically active compounds and pharmaceuticals, in good yields. |
| تدمد: | 1463-9270 1463-9262 |
| URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_________::a75a7055623750833b1e7abf470ef159 https://doi.org/10.1039/d0gc01360a |
| حقوق: | CLOSED |
| رقم الأكسشن: | edsair.doi...........a75a7055623750833b1e7abf470ef159 |
| قاعدة البيانات: | OpenAIRE |
| تدمد: | 14639270 14639262 |
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