The effect of nitrogen flow rate on Acrawax C decomposition and its removal during sintering of Alumix 431D grade powder
العنوان: | The effect of nitrogen flow rate on Acrawax C decomposition and its removal during sintering of Alumix 431D grade powder |
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المؤلفون: | Jan Kazior, M. Laska, T. Pieczonka |
المصدر: | Powder Metallurgy. 61:149-156 |
بيانات النشر: | Informa UK Limited, 2017. |
سنة النشر: | 2017 |
مصطلحات موضوعية: | Materials science, 020502 materials, Metallurgy, Metals and Alloys, Sintering, 02 engineering and technology, 021001 nanoscience & nanotechnology, Condensed Matter Physics, medicine.disease_cause, Mass spectrometry, Decomposition, Nitrogen flow rate, Soot, Volumetric flow rate, 0205 materials engineering, Mechanics of Materials, Materials Chemistry, Ceramics and Composites, medicine, Lubricant, 0210 nano-technology, Thermal analysis |
الوصف: | Alumix 431D pre-alloyed powder (ECKA Granules GmbH) containing 1.5 mass% of Acrawax C was used to study the effect of nitrogen flow rate on delubrication and sintering evolution. Mass loss of compacts during heating was controlled by the TG method using a STA Netzsch apparatus coupled with a mass spectrometer. The latter was used to identify the volatile lubricant’s decomposition products. Macro- and microstructural observations of sintered compacts were also performed. The results documented a strong influence of nitrogen flow rate on delubrication and thus on the sintering behaviour of examined powder. High nitrogen flow rate is required to produce the desired sintered compacts. In contrast, at low nitrogen velocity, the lubricant removal is not complete, which leads to the formation of carbonaceous residuals in the form of soot, which in turn significantly impedes densification and deteriorates the sintered products. |
تدمد: | 1743-2901 0032-5899 |
URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_________::d924fc55f28bb00910b811bf7b99cbc3 https://doi.org/10.1080/00325899.2017.1410999 |
رقم الأكسشن: | edsair.doi...........d924fc55f28bb00910b811bf7b99cbc3 |
قاعدة البيانات: | OpenAIRE |
تدمد: | 17432901 00325899 |
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