Simultaneous determination of the herbicide bixlozone and its metabolites in plant and animal samples by liquid chromatography–tandem mass spectrometry
| العنوان: | Simultaneous determination of the herbicide bixlozone and its metabolites in plant and animal samples by liquid chromatography–tandem mass spectrometry |
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| المؤلفون: | Rong Liu, Zenglong Chen, Congdi Li, Li Li, Longfei Yuan, Yujian He, Wei Li, Dongmei Qin |
| المصدر: | Journal of Separation Science. 44:822-832 |
| بيانات النشر: | Wiley, 2021. |
| سنة النشر: | 2021 |
| مصطلحات موضوعية: | Meat, Wheat flour, Filtration and Separation, Mass spectrometry, Quechers, 01 natural sciences, Analytical Chemistry, Human health, 0404 agricultural biotechnology, Solanum lycopersicum, Tandem Mass Spectrometry, Liquid chromatography–mass spectrometry, Animals, Chromatography, High Pressure Liquid, Ovum, Detection limit, Residue (complex analysis), Chromatography, Herbicides, Chemistry, 010401 analytical chemistry, 04 agricultural and veterinary sciences, 040401 food science, 0104 chemical sciences, 2 × 2 real matrices, Milk, Malus, Cucumis sativus |
| الوصف: | Tracing the herbicide bixlozone and its metabolites in food is necessary to assess their risks to human health. In the study, a rapid and effective analytical method using the quick, easy, cheap, effective, rugged, and safe (QuEChERS) method for the simultaneous determination of bixlozone and its metabolites (2,4-dichlorobenzoic acid, 3-hydroxy-propanamide-bixlozone, and 5'-hydroxy-bixlozone) in plant and animal samples (tomato, cucumber, apple, wheat flour, meat, milk, and egg) was developed based on ultra-performance liquid chromatography-tandem mass spectrometry. The method was validated based on the linearity (R2 > 0.99), sensitivity (limit of quantification = 0.01 mg/kg), recovery (70.2%-115.1%), and precision (intra-day 1.2%-17.6%, inter-day 0.3%-16.0%). Detection was achieved within 6.0 min. The method is reliable for the determination of four target compounds in all seven matrices. The satisfactory validation criteria and successful application show that the proposed methodology is suitable for the detection of four target compounds in real matrices. This article is protected by copyright. All rights reserved. |
| تدمد: | 1615-9314 1615-9306 |
| URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_dedup___::4b05b32d509704127136c3f931a48015 https://doi.org/10.1002/jssc.202000992 |
| حقوق: | CLOSED |
| رقم الأكسشن: | edsair.doi.dedup.....4b05b32d509704127136c3f931a48015 |
| قاعدة البيانات: | OpenAIRE |
| تدمد: | 16159314 16159306 |
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