Flow-through compression cell for small-angle and ultra-small-angle neutron scattering measurements

التفاصيل البيبلوغرافية
العنوان: Flow-through compression cell for small-angle and ultra-small-angle neutron scattering measurements
المؤلفون: Rex P. Hjelm, Jason E. Heath, Daniel Olds, Luke P. Frash, Mei Ding, Hongwu Xu, Marilyn E. Hawley, Mark A. Taylor, Thomas A. Dewers, J. G. Barker
المصدر: The Review of scientific instruments. 89(5)
سنة النشر: 2018
مصطلحات موضوعية: Materials science, 010304 chemical physics, Effective stress, Neutron radiation, Neutron scattering, 010502 geochemistry & geophysics, 01 natural sciences, Small-angle neutron scattering, law.invention, law, 0103 physical sciences, Nano, Neutron, Hydrostatic equilibrium, Composite material, Porosity, Instrumentation, 0105 earth and related environmental sciences
الوصف: In situ measurements of geological materials under compression and with hydrostatic fluid pressure are important in understanding their behavior under field conditions, which in turn provides critical information for application-driven research. In particular, understanding the role of nano- to micro-scale porosity in the subsurface liquid and gas flow is critical for the high-fidelity characterization of the transport and more efficient extraction of the associated energy resources. In other applications, where parts are produced by the consolidation of powders by compression, the resulting porosity and crystallite orientation (texture) may affect its in-use characteristics. Small-angle neutron scattering (SANS) and ultra SANS are ideal probes for characterization of these porous structures over the nano to micro length scales. Here we show the design, realization, and performance of a novel neutron scattering sample environment, a specially designed compression cell, which provides compressive stress and hydrostatic pressures with effective stress up to 60 MPa, using the neutron beam to probe the effects of stress vectors parallel to the neutron beam. We demonstrate that the neutron optics is suitable for the experimental objectives and that the system is highly stable to the stress and pressure conditions of the measurements.
تدمد: 1089-7623
URL الوصول: https://explore.openaire.eu/search/publication?articleId=doi_dedup___::828b52a3175060726d1788e15f8a2a08
https://pubmed.ncbi.nlm.nih.gov/29864818
حقوق: OPEN
رقم الأكسشن: edsair.doi.dedup.....828b52a3175060726d1788e15f8a2a08
قاعدة البيانات: OpenAIRE