In situ 4D tomography image analysis framework to follow sintering within 3D‐printed glass scaffolds
العنوان: | In situ 4D tomography image analysis framework to follow sintering within 3D‐printed glass scaffolds |
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المؤلفون: | Julian R. Jones, Achintha I. Kondarage, Peter D. Lee, Amy Nommeots-Nomm, Angelo Karunaratne, Thilina Dulantha Lalitharatne, Gowsihan Poologasundarampillai, Nuwan D. Nanayakkara |
المساهمون: | National Institute for Health Research |
المصدر: | Journal of the American Ceramic Society. 105:1671-1684 |
بيانات النشر: | Wiley, 2021. |
سنة النشر: | 2021 |
مصطلحات موضوعية: | Technology, Materials science, Materials Science, Sintering, law.invention, CERAMIC PARTS, image analysis, DEFORMATION, law, Materials Chemistry, Ceramic, Composite material, 0912 Materials Engineering, Porosity, Materials, Shrinkage, X-ray computed tomography, REPAIR, sintering, Science & Technology, Tomographic reconstruction, bioactive glass, POROSITY, EVOLUTION, Metrology, Bioactive glass, visual_art, bioceramics, Ceramics and Composites, visual_art.visual_art_medium, Tomography, Materials Science, Ceramics, BEHAVIOR, 0913 Mechanical Engineering |
الوصف: | We propose a novel image analysis framework to automate analysis of X-ray microtomography images of sintering ceramics and glasses, using open-source toolkits and machine learning. Additive manufacturing (AM) of glasses and ceramics usually requires sintering of green bodies. Sintering causes shrinkage, which presents a challenge for controlling the metrology of the final architecture. Therefore, being able to monitor sintering in 3D over time (termed 4D) is important when developing new porous ceramics or glasses. Synchrotron X-ray tomographic imaging allows in situ, real-time capture of the sintering process at both micro and macro scales using a furnace rig, facilitating 4D quantitative analysis of the process. The proposed image analysis framework is capable of tracking and quantifying the densification of glass or ceramic particles within multiple volumes of interest (VOIs) along with structural changes over time using 4D image data. The framework is demonstrated by 4D quantitative analysis of bioactive glass ICIE16 within a 3D-printed scaffold. Here, densification of glass particles within 3 VOIs were tracked and quantified along with diameter change of struts and interstrut pore size over the 3D image series, delivering new insights on the sintering mechanism of ICIE16 bioactive glass particles in both micro and macro scales |
تدمد: | 1551-2916 0002-7820 |
URL الوصول: | https://explore.openaire.eu/search/publication?articleId=doi_dedup___::d82ea18fde38b07bd16955ad88176972 https://doi.org/10.1111/jace.18182 |
حقوق: | OPEN |
رقم الأكسشن: | edsair.doi.dedup.....d82ea18fde38b07bd16955ad88176972 |
قاعدة البيانات: | OpenAIRE |
تدمد: | 15512916 00027820 |
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