دورية أكاديمية
Production of copper nanoparticles using alpha-amylase enzyme by an electrochemical deposition method
| العنوان: | Production of copper nanoparticles using alpha-amylase enzyme by an electrochemical deposition method |
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| المؤلفون: | Neamah Hadi, Mohammad Hafiz, F. Sayyid, Wan Wan Isahak |
| المصدر: | Engineering and Technology Journal, Vol 42, Iss 6, Pp 768-782 (2024) |
| بيانات النشر: | Unviversity of Technology- Iraq, 2024. |
| سنة النشر: | 2024 |
| المجموعة: | LCC:Science LCC:Technology |
| مصطلحات موضوعية: | alpha amylase enzyme, copper powder, electrodeposition process, current density, current efficiency, Science, Technology |
| الوصف: | This study aims to explain the effect of adding the bioactive substance (alpha enzyme) to the electrolyte solution using electrochemical deposition. Through which copper nanoparticles are manufactured, the originality of the research lies in the presence of this addition as a new method in manufacturing nanoparticles in an electrochemical manner, as the alpha-amylase enzyme is extracted from camel saliva, and the product has been diagnosed using (EDX) and scanning electron microscope (FE-SEM) techniques. , Dynamic Light Scattering (DLS) technology, and Zeta potential. The proposed method is an easy, inexpensive, and environmentally friendly method where the alpha enzyme was used as a feedstock at concentrations of (0.25, 0.50, 0.57, and 1) g added to a solution containing the ideal sample obtained through the electrochemical precipitation process before adding the enzyme, as the solution before The addition process contains concentrated sulfuric acid (H2SO4) at concentrations of (20, 30, 40, 50 and 60) g/ml. The regular shape and stable distribution can be observed after the addition compared to the shape of the particles before the addition in terms of shape and size. The process was carried out under constant conditions, including the current. Direct, voltage and temperature, and after the addition process, sulfuric acid was dispensed with, while the process conditions with the addition were at a temperature of 37 degrees Celsius and an incubation period that lasted a full hour before the electrodeposition process was carried out in accordance with the enzyme activity conditions, where a nanosized copper powder of a granular size was obtained. Approximately 44 nanometers. It is worth noting that the nanoparticle size was modulated using the experimental conditions, e.g., pH, reducing step, enzyme amount, or incubation time. This controlled synthesis allows the preparation of CuNP bionanoparticles at Cu 3.13 powder at a concentration of 80 g CuSO4 + 0.50 α-amylase. |
| نوع الوثيقة: | article |
| وصف الملف: | electronic resource |
| اللغة: | English |
| تدمد: | 1681-6900 2412-0758 |
| Relation: | https://etj.uotechnology.edu.iq/article_183248_f23eec1632e6e238082f1117d276a403.pdf; https://doaj.org/toc/1681-6900; https://doaj.org/toc/2412-0758 |
| DOI: | 10.30684/etj.2024.146236.1674 |
| URL الوصول: | https://doaj.org/article/2e399be5886a49c5bd9a21f28225e7cc |
| رقم الأكسشن: | edsdoj.2e399be5886a49c5bd9a21f28225e7cc |
| قاعدة البيانات: | Directory of Open Access Journals |
Full Text Finder | تدمد: | 16816900 24120758 |
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| DOI: | 10.30684/etj.2024.146236.1674 |