دورية أكاديمية
Effect of Sterilization on the Properties of a Bioactive Hybrid Coating Containing Hydroxyapatite
| العنوان: | Effect of Sterilization on the Properties of a Bioactive Hybrid Coating Containing Hydroxyapatite |
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| المؤلفون: | E. K. K. Baldin, C. F. Malfatti, V. Rodói, R. N. Brandalise |
| المصدر: | Advances in Materials Science and Engineering, Vol 2019 (2019) |
| بيانات النشر: | Wiley, 2019. |
| سنة النشر: | 2019 |
| المجموعة: | LCC:Materials of engineering and construction. Mechanics of materials |
| مصطلحات موضوعية: | Materials of engineering and construction. Mechanics of materials, TA401-492 |
| الوصف: | The objective of this study was to evaluate the influence of sterilization on a hybrid coating obtained from a sol composed of alkoxysilane tetraethoxysilane (TEOS) and organoalkoxysilane methyltriethoxysilane (MTES) containing 10% (mass) of hydroxyapatite particles. The coating was obtained by dip coating, by applying two layers (protective/bioactive), which were cured at different temperatures (450°C and 60°C). The effects of sterilization on the superficial, electrochemical, bioactive, and mechanical properties of the coating were evaluated by performing different sterilization processes, namely, steam autoclave, hydrogen peroxide plasma, and ethylene oxide. Subsequently, the coating was characterized by using scanning electron microscopy (SEM/FEG), and FTIR measurements were performed to characterize the chemical structure. The bioactivity and degradability of the coating were analyzed by mass variation after immersion in SBF and X-ray diffraction (XRD) analysis. The electrochemical behavior was assessed by open circuit potential (OCP) and potentiodynamic polarization curves and the mechanical behavior by wear resistance. Results showed that all sterilization processes caused significant morphological changes in the hybrid coating. The autoclaved sample presented the highest structural chemical changes, and, consequently, the highest degradability, even though it had a superior bioactive behavior in relation to the other samples. In addition, the sterilization processes influenced the electrochemical behavior of the hybrid coating and altered the mechanical resistance to abrasion, thus presenting lower wear performance in relation to the nonsterilized sample. |
| نوع الوثيقة: | article |
| وصف الملف: | electronic resource |
| اللغة: | English |
| تدمد: | 1687-8434 1687-8442 |
| Relation: | https://doaj.org/toc/1687-8434; https://doaj.org/toc/1687-8442 |
| DOI: | 10.1155/2019/8593193 |
| URL الوصول: | https://doaj.org/article/3ce2dcf45d444026a9e1338de51d3899 |
| رقم الأكسشن: | edsdoj.3ce2dcf45d444026a9e1338de51d3899 |
| قاعدة البيانات: | Directory of Open Access Journals |
Full Text Finder | تدمد: | 16878434 16878442 |
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| DOI: | 10.1155/2019/8593193 |