دورية أكاديمية
أعرض في EDS

SFX analysis of non-biological polycrystalline samples

التفاصيل البيبلوغرافية
العنوان: SFX analysis of non-biological polycrystalline samples
المؤلفون: Tao Zhang, Shifeng Jin, Yuanxin Gu, Yao He, Ming Li, Yang Li, Haifu Fan
المصدر: IUCrJ, Vol 2, Iss 3, Pp 322-326 (2015)
بيانات النشر: International Union of Crystallography, 2015.
سنة النشر: 2015
المجموعة: LCC:Crystallography
مصطلحات موضوعية: serial crystallography, X-ray powder diffraction, phase identification, structure solution, Crystallography, QD901-999
الوصف: Serial femtosecond crystallography (SFX) is capable of collecting three-dimensional single-crystal diffraction data using polycrystalline samples. This may dramatically enhance the power of X-ray powder diffraction. In this paper a test has been performed using simulated diffraction patterns. The test sample is a mixture of two zeolites with crystal grain sizes from 100 to 300 nm. X-ray diffraction snapshots by SFX were simulated and processed using the program suite CrystFEL. Identification according to the primitive unit-cell volume determined from individual snapshots was able to separate the whole set of snapshots into two subsets, which correspond to the two zeolites in the sample. Monte Carlo integration in CrystFEL was then applied to them separately. This led to two sets of three-dimensional single-crystal diffraction intensities, based on which crystal structures of the two zeolites were solved easily by direct methods implemented in the program SHELXD.
نوع الوثيقة: article
وصف الملف: electronic resource
اللغة: English
تدمد: 2052-2525
20522525
Relation: http://scripts.iucr.org/cgi-bin/paper?S2052252515002146; https://doaj.org/toc/2052-2525
DOI: 10.1107/S2052252515002146
URL الوصول: https://doaj.org/article/64b7557498a1460789fac9dda3753c9e
رقم الأكسشن: edsdoj.64b7557498a1460789fac9dda3753c9e
قاعدة البيانات: Directory of Open Access Journals
الوصف
تدمد:20522525
DOI:10.1107/S2052252515002146