دورية أكاديمية
Determination of Eight Amide Herbicide Residues in Animal-derived Foods by Gas Chromatography-Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry
| العنوان: | Determination of Eight Amide Herbicide Residues in Animal-derived Foods by Gas Chromatography-Atmospheric Pressure Chemical Ionization-Tandem Mass Spectrometry |
|---|---|
| المؤلفون: | YANG Zhijin, LIN Binbin, HUANG Xuliang, CHEN Qianni, LIN Xiaolian, LAN Yanshan |
| المصدر: | Shipin Kexue, Vol 44, Iss 22, Pp 373-379 (2023) |
| بيانات النشر: | China Food Publishing Company, 2023. |
| سنة النشر: | 2023 |
| المجموعة: | LCC:Food processing and manufacture |
| مصطلحات موضوعية: | atmospheric pressure chemical ionization, gas chromatography-tandem mass spectrometry, amide herbicides, animal-derived food, Food processing and manufacture, TP368-456 |
| الوصف: | A gas chromatography-atmospheric pressure chemical ionization-tandem mass spectrometry (GC-APCI-MS/MS) method was established for the determination of the residues of eight amide herbicides (alachlor, acetochlor, propichlor, butachlor, dichlorochlor, pyrazolam, dimethochlor and metolachlor) in animal-derived foods. The sample pretreatment process involved acetonitrile extraction and enhanced matrix removal (EMR)-lipid cleanup, and ethyl acetate was used to dilute the purified acetonitrile extract instead of solvent conversion. The detection was performed with APCI in the positive ion mode using multi-reaction monitoring (MRM). The results showed that the average recoveries of the eight amide herbicides in spiked pork, pig liver, egg and milk matrices were 63.3%–108%, with relative standard deviation (RSD) 2.51%–13.8%. The limit of detection (LOD) was 0.029–1.3 µg/kg, the limit of quantitation (LOQ) was 0.095–4.2 µg/kg, and the matrix effect was −11%–12%. This method can effectively reduce the matrix effect, and is simple, efficient, accurate, sensitive, and suitable for the rapid quantitative determination of the eight amide herbicides in animal-derived foods. |
| نوع الوثيقة: | article |
| وصف الملف: | electronic resource |
| اللغة: | English Chinese |
| تدمد: | 1002-6630 |
| Relation: | https://www.spkx.net.cn/fileup/1002-6630/PDF/2023-44-22-045.pdf; https://doaj.org/toc/1002-6630 |
| DOI: | 10.7506/spkx1002-6630-20230219-172 |
| URL الوصول: | https://doaj.org/article/ab43aa9f853b46a482a739b0fcbcbe02 |
| رقم الأكسشن: | edsdoj.b43aa9f853b46a482a739b0fcbcbe02 |
| قاعدة البيانات: | Directory of Open Access Journals |
Full Text Finder | تدمد: | 10026630 |
|---|---|
| DOI: | 10.7506/spkx1002-6630-20230219-172 |