دورية أكاديمية
Characterization of γ′ Precipitates in Cast Ni-Based Superalloy and Their Behaviour at High-Homologous Temperatures Studied by TEM and in Situ XRD
العنوان: | Characterization of γ′ Precipitates in Cast Ni-Based Superalloy and Their Behaviour at High-Homologous Temperatures Studied by TEM and in Situ XRD |
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المؤلفون: | Łukasz Rakoczy, Ondrej Milkovič, Bogdan Rutkowski, Rafał Cygan, Małgorzata Grudzień-Rakoczy, František Kromka, Anna Zielińska-Lipiec |
المصدر: | Materials, Vol 13, Iss 10, p 2397 (2020) |
بيانات النشر: | MDPI AG, 2020. |
سنة النشر: | 2020 |
المجموعة: | LCC:Technology LCC:Electrical engineering. Electronics. Nuclear engineering LCC:Engineering (General). Civil engineering (General) LCC:Microscopy LCC:Descriptive and experimental mechanics |
مصطلحات موضوعية: | misfit, in situ XRD, lattice parameter, STEM, gamma prime, dissolution, Technology, Electrical engineering. Electronics. Nuclear engineering, TK1-9971, Engineering (General). Civil engineering (General), TA1-2040, Microscopy, QH201-278.5, Descriptive and experimental mechanics, QC120-168.85 |
الوصف: | In situ X-ray diffraction and transmission electron microscopy has been used to investigate René 108 Ni-based superalloy after short-term annealing at high-homologous temperatures. Current work is focused on characterisation of γ′ precipitates, their volume fraction, evolution of the lattice parameter of γ and γ′ phases and misfit parameter of γ′ in the matrix. Material in the initial condition is characterised by a high-volume fraction (over 63%) of γ′ precipitates. Irregular distribution of alloying elements was observed. Matrix channels were strongly enriched in Cr, Co, W and Mo, whereas precipitates contain large amount of Al, Ti, Ta and Hf. Exposure to high-homologous temperatures in the range 1100–1250 °C led to the dissolution of the precipitates, which influenced the change of lattice parameter of both γ and γ′ phases. The lattice parameter of the matrix continuously grew during holding at high temperatures, which had a dominant influence on the more negative misfit coefficient. |
نوع الوثيقة: | article |
وصف الملف: | electronic resource |
اللغة: | English |
تدمد: | 13102397 1996-1944 |
Relation: | https://www.mdpi.com/1996-1944/13/10/2397; https://doaj.org/toc/1996-1944 |
DOI: | 10.3390/ma13102397 |
URL الوصول: | https://doaj.org/article/f962bd788ed844b8bf58990eb40bc3eb |
رقم الأكسشن: | edsdoj.f962bd788ed844b8bf58990eb40bc3eb |
قاعدة البيانات: | Directory of Open Access Journals |
تدمد: | 13102397 19961944 |
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DOI: | 10.3390/ma13102397 |